Toluene → Benzene, [2-(1-methylethoxy)ethyl]-

HRID 1065058ノート

反応式

HRID 1065058 の反応式
C1(C)C=CC=CC=1.C(OC(=O)CC)(=O)CC.C(OC(=O)CC)(=O)CC.C1(C)C=CC=CC=1.C1(CCO)C=CC=CC=1.[CH:42]([O:45][CH2:46][CH2:47][C:48]1[CH:53]=[CH:52][CH:51]=[CH:50][CH:49]=1)([CH3:44])[CH3:43]>O>[CH:42]([O:45][CH2:46][CH2:47][C:48]1[CH:49]=[CH:50][CH:51]=[CH:52][CH:53]=1)([CH3:44])[CH3:43]

参加物

5

反応物 3

HCID 1140TolueneHCID 31263Propionic anhydrideHCID 86738357HCID 86738357、化合物

生成物 1

HCID 106442Benzene, [2-(1-methylethoxy)ethyl]-

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

To the toluene mixture is added 260 grams of propionic anhydride and the propionic anhydride/toluene/phenylethyl alcohol/isopropyl phenethylether mixture is then refluxed for a period of 30 minutes. The reaction mass is then cooled down and one liter of water is added thereto. The reaction mass is then washed with 50% caustic followed by saturated sodium chloride and then neutralized with saturated sodium bicarbonate.

後処理

  1. temperatureThe reaction mass is then cooled down
  2. washThe reaction mass is then washed with 50%

出典と根拠

ORDレコード
ord-c202b076e4da4d23ac53595b4b225995
出典データセット
uspto-grants-1982_05
特許番号
US04328206

反応ノート

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