戻る
化工社化工社 化学情報印刷レポート · 研究参考用
HRID 1065179作成日:2026年10月27日

Isobutylene → 1-tert-Butyl-4-(3-chloro-2-methylpropyl)benzene

https://huagongshe.com/reaction/1065179

反応式

関与物質

役割名称HCID仕込み量
反応物IsobutyleneHCID 8255—
反応物Hydrofluoric AcidHCID 14917—
反応物(3-Chloro-2-methylpropyl)benzeneHCID 13510156—
生成物1-tert-Butyl-4-(3-chloro-2-methylpropyl)benzeneHCID 13251817—
生成物(3-Chloro-2-methylpropyl)benzeneHCID 13510156—

反応手順

20 parts by weight of isobutene are passed into a mixture of 68 parts by weight of 2-methyl-3-phenylpropyl chloride and 3 parts by weight of hydrogen fluoride at 0° C. The mixture is then stirred for 12 hours at room temperature. The crude product is washed with water, dried over Na2CO3 and distilled. 36 parts by weight of 2-methyl-3-phenylpropyl chloride, boiling point 105° C./16 mm Hg and 32 parts by weight of 2-methyl-3-(p-tert.-butylphenyl)-propyl chloride, boiling point 80° C.-81° C./0.02 mm Hg, are obtained.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04328380
出典データセットuspto-grants-1982_05
ORD IDord-5821a7df913a4bd5b7c6ff5bdf662702
出典メモuspto-grants-1982_05