化工社化工社 化学情報印刷レポート · 研究参考用
Acetic Acid → Dodecanedioic Acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetic Acid | HCID 176 | — |
| 反応物 | Cyclododecene, (E)- | HCID 15164 | — |
| 反応物 | 3a,4,5,7a-Tetrahydro-2-benzofuran-1,3-dione | HCID 12726601 | — |
| 生成物 | Dodecanedioic Acid | HCID 12736 | 94% |
反応手順
The co-oxidation reaction was carried out in a manner as described in Example 1, except that cyclododecene was used in lieu of cis-Δ4 -tetrahydrophthalic anhydride. Acetic acid was obtained at a yield of 95% and 1,10-dicarboxy decane was obtained at a yield of 94%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04331608 |
| 出典データセット | uspto-grants-1982_05 |
| ORD ID | ord-c134627c84a54450bdb1e8d5cc547349 |
| 出典メモ | uspto-grants-1982_05 |