3-Chloro-5-(trifluoromethyl)-2-pyridinamine → N-(3-chloro-5-trifluoromethyl-2-pyridyl)-2,4-dinitro-3-methoxy-6-trifluoromethylaniline

HRID 1065779

反応式

HRID 1065779 の反応式
[NH2:1][C:2]1[C:7]([Cl:8])=[CH:6][C:5]([C:9]([F:12])([F:11])[F:10])=[CH:4][N:3]=1.[N+:13]([C:16]1[C:21]([O:22][CH3:23])=[C:20]([N+:24]([O-:26])=[O:25])[CH:19]=[C:18]([C:27]([F:30])([F:29])[F:28])[C:17]=1Cl)([O-:15])=[O:14]>>[Cl:8][C:7]1[C:2]([NH:1][C:17]2[C:18]([C:27]([F:30])([F:29])[F:28])=[CH:19][C:20]([N+:24]([O-:26])=[O:25])=[C:21]([O:22][CH3:23])[C:16]=2[N+:13]([O-:15])=[O:14])=[N:3][CH:4]=[C:5]([C:9]([F:12])([F:10])[F:11])[CH:6]=1

参加物

3

反応物 2

HCID 6072483-Chloro-5-(trifluoromethyl)-2-pyridinamineHCID 205385892,4-Dinitro-3-methoxy-6-trifluoromethylchlorobenzene

生成物 1

HCID 13043913N-(3-chloro-5-trifluoromethyl-2-pyridyl)-2,4-dinitro-3-methoxy-6-trifluoromethylaniline

実験手順

In accordance with the process of Preparation 8 except using 1.9 g. of 2-amino-3-chloro-5-trifluoromethylpyridine and 2.8 g. of 2,4-dinitro-3-methoxy-6-trifluoromethylchlorobenzene, the reaction was carried out for 3 hours. The reaction mixture was treated as the process of Preparation 6 to obtain 1.4 g. of the object oily compound.

後処理

  1. customIn accordance with the process of Preparation 8
  2. additionThe reaction mixture was treated as the process of Preparation 6
  3. customto obtain 1.4 g

出典と根拠

ORDレコード
ord-080000c8c2ec4c20a9611b75fc2e1c26
出典データセット
uspto-grants-1982_05
特許番号
US04331670

関連ノート

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