関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Sulfuric Acid | HCID 1118 | — |
| 反応物 | Acetic Anhydride | HCID 7918 | — |
| 反応物 | Methyl 3-Hydroxy-2-methylene-3-phenylpropionate | HCID 9942369 | — |
| 生成物 | Methyl 2-[(acetyloxy)methyl]-3-phenylprop-2-enoate | HCID 53678280 | 100.8% |
反応手順
Methyl 3-hydroxy-2-methylene-3-phenylpropionate (1.7836 g, 9.279 mmols) was dissolved in 1.75 ml (18.55 mmols) of acetic anhydride, and 0.03 ml of sulfuric acid were added thereto. The mixture was stirred at 100° C. for 4 hours. After the completion of the reaction, the reaction solution was concentrated under reduced pressure to obtain 2.1917 g of a crude product of the above title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US06242635B1 |
|---|
| 出典データセット | uspto-grants-2001_06 |
|---|
| ORD ID | ord-bf7fac68b2be4e1680fe67d00927874a |
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| 出典メモ | uspto-grants-2001_06 |
|---|
