Butylimidazole → 1-Butyl-3-methylimidazolium tetrafluoroborate

HRID 1067042

反応式

HRID 1067042 の反応式
[F:1][B-:2]([F:5])([F:4])[F:3].[CH3:6][O+](C)C.[CH2:10]([N:14]1[CH:18]=[CH:17][N:16]=[CH:15]1)[CH2:11][CH2:12][CH3:13]>ClCCCl>[F:1][B-:2]([F:5])([F:4])[F:3].[CH3:6][N+:16]1[CH:17]=[CH:18][N:14]([CH2:10][CH2:11][CH2:12][CH3:13])[CH:15]=1

参加物

4

反応物 2

HCID 61347ButylimidazoleHCID 2735153Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1)

生成物 1

HCID 27341781-Butyl-3-methylimidazolium tetrafluoroborate

試薬・触媒・溶媒 1

HCID 111,2-Dichloroethane溶媒2 回

実験手順

The procedure of Example 2 was followed. 3 g of trimethyloxonium tetrafluoroborate in suspension in 10 ml of 1,2-dichloroethane was added to 2.7 ml of N-butylimidazole in 10 ml of 1,2-dichloroethane. The mixture was stirred for 4 hours at room temperature. The remaining solvent was evaporated off under vacuum using a vane pump. A colorless liquid was obtained.

後処理

  1. customThe remaining solvent was evaporated off under vacuum
  2. customA colorless liquid was obtained

出典と根拠

ORDレコード
ord-83f6c74419bd4ec6866c10e468d98ae4
出典データセット
uspto-grants-2001_06
特許番号
US06245918B1

関連ノート

読み込み中…