反応式
C(P(CCCC)CCCC)CCC.Cl[CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20].[Cl:21][SiH:22]([Cl:24])[Cl:23]>>[CH2:15]([Si:22]([Cl:24])([Cl:23])[Cl:21])[CH2:16][CH2:17][CH2:18][CH2:19][CH3:20]参加物
4
反応条件
- 温度
- 150 °C
実験手順
In a 25 ml oven dried stainless steel tube, 0.15 g (0.75 mmol) of tri-n-butylphosphine, 0.90 g (7.5 mmol) of 1-chlorohexane, and 5.08 g (37.5 mmol) of trichlorosilane were added under a dry nitrogen atmosphere. After sealing the cylinder with a valve, the reactor was maintained at 150° C. for 12 hrs. The resulting mixture was distilled to yield 1.1 g of n-hexyltrichlorosilane (bp; 215-219° C., yield; 65%).
後処理
- distillationThe resulting mixture was distilled
出典と根拠
- ORDレコード
- ord-2ec5a80fe7254d0484b7a147c6ae5bb6
- 出典データセット
- uspto-grants-2001_06
- 特許番号
- US06251057B1
関連ノート
読み込み中…