2-Thiophenecarboxaldehyde → 7-(Thiophen-2-yl)carbonylimidazo[5,1-b]thiazole

反応式

I[C:2]1[N:3]=[CH:4][N:5]2[CH:9]=[CH:8][S:7][C:6]=12.[S:10]1[CH:14]=[CH:13][CH:12]=[C:11]1[CH:15]=[O:16]>>[S:10]1[CH:14]=[CH:13][CH:12]=[C:11]1[C:15]([C:2]1[N:3]=[CH:4][N:5]2[CH:9]=[CH:8][S:7][C:6]=12)=[O:16]

参加物

反応物 2

HCID 73642-Thiophenecarboxaldehyde

HCID 177737777-Iodoimidazo[5,1-B]thiazole

生成物 1

HCID 223903097-(Thiophen-2-yl)carbonylimidazo[5,1-b]thiazole

実験手順

7-(Thiophen-2-yl)carbonylimidazo[5,1-b]thiazole (1.37 g) was prepared in the same manner as in step a) of Synthesis Example 3, except that 1.50 g of 7-iodoimidazo[5,1-b]thiazole and 0.561 ml of thiophene-2-aldehyde were used as the starting compounds.

後処理

customof Synthesis Example 3

出典と根拠

ORDレコード: ord-9189a57c65744dba9b6172fb003ec99f
出典データセット: uspto-grants-2005_06
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US06908913B2

反応ノート

読み込み中…