化工社化工社 化学情報印刷レポート · 研究参考用
Dibutylstannane → Bis(2-acetoxyethyl)dibutyltin
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dibutylstannane | HCID 6513 | — |
| 反応物 | Vinyl Acetate | HCID 7904 | — |
| 溶媒 | Cyclohexane | HCID 8078 | — |
| 生成物 | Bis(2-acetoxyethyl)dibutyltin | HCID 14512231 | — |
反応手順
2.349 g (0.01 mole) of dibutyltin dihydride, 1.722 g (0.02 mole) of distilled vinyl acetate and 2 g of anhydrous cyclohexane were introduced into a Pyrex® vessel thermostated at 25° C. The solution was exposed to ultraviolet rays for 3 hours. The cyclohexane was then removed under vacuum at ambient temperature. The expected product was obtained pure in quantitative yield.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04970115 |
| 出典データセット | uspto-grants-1990_11 |
| ORD ID | ord-de52867de7ff4041b8ea5da112312347 |
| 出典メモ | uspto-grants-1990_11 |