Vinyl Acetate → HCID 14512238、化合物
反応式
[C:1]1([SnH2:7][C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C:14]([O:17][CH:18]=[CH2:19])(=[O:16])[CH3:15]>C1CCCCC1>[C:14]([O:17][CH2:18][CH2:19][Sn:7]([CH2:19][CH2:18][O:17][C:14](=[O:16])[CH3:15])([C:1]1[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1)[C:8]1[CH:9]=[CH:10][CH:11]=[CH:12][CH:13]=1)(=[O:16])[CH3:15]参加物
4
実験手順
Diphenyltin dihydride and vinyl acetate were introduced in stoichiometric amount into a Pyrex® tube containing anhydrous cyclohexane. The reaction mixture was exposed to ultraviolet rays for 1 hour at 30° C. The solvent was then removed under vacuum at ambient temperature. The product, obtained quantitatively, had the following formula:
後処理
- customfor 1 hour
- customat 30° C
- customThe solvent was then removed under vacuum at ambient temperature
- customThe product, obtained quantitatively
出典と根拠
- ORDレコード
- ord-73c59147aab5472eb28b9287a637ccca
- 出典データセット
- uspto-grants-1990_11
- 特許番号
- US04970115
反応ノート
読み込み中…