化工社化工社 化学情報印刷レポート · 研究参考用
Benzyl Chloride → Benzyl 4-Hydroxybenzoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzyl Chloride | HCID 7503 | — |
| 反応物 | Sodium 4-hydroxybenzoate | HCID 16219477 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | Benzyl 4-Hydroxybenzoate | HCID 7180 | 74% |
反応手順
Sodium p-hydroxybenzoate (64 g) and 51 g of benzyl chloride were added to 150 g of dimethylformamide, and reacted at 100° C. for 3 hours. Benzyl p-hydroxybenzoate was obtained in a yield of 74%. The ratio of benzyl p-benzyloxybenzoate, a by-product, formed was 10%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04973737 |
| 出典データセット | uspto-grants-1990_11 |
| ORD ID | ord-8ad97fb84fbe49b499868575a5da03c6 |
| 出典メモ | uspto-grants-1990_11 |