2,6-Naphthalenedicarbonyl dichloride → 2-Naphthoyl chloride

HRID 1074303

反応式

HRID 1074303 の反応式
FC(F)(F)CCCCCCC1(C2C=CC(O)=CC=2)C=CC(C([O-])=O)=CC1.[CH:27]1[C:36]2[C:31](=[CH:32][C:33]([C:37]([Cl:39])=[O:38])=[CH:34][CH:35]=2)[CH:30]=[CH:29][C:28]=1C(Cl)=O>C(N(CC)CC)C>[CH:32]1[C:31]2[C:36](=[CH:27][CH:28]=[CH:29][CH:30]=2)[CH:35]=[CH:34][C:33]=1[C:37]([Cl:39])=[O:38]

参加物

4

反応物 2

HCID 34855962,6-Naphthalenedicarbonyl dichlorideHCID 867443591-Trifluoroheptyl-4'-hydroxybiphenyl-4-carboxylate

生成物 1

HCID 752462-Naphthoyl chloride

試薬・触媒・溶媒 1

HCID 8471Triethylamine溶媒

実験手順

The compound (III) is reacted with 2,6-naphthalene-dicarboxylic acid dichloride in the presence of triethyl amine to obtain 6-[3-trifluoromethylheptyloxycarbonyl)-biphenyl-4-oxycarbonyl]-naphthalene-2-carboxylic acid chloride (IV).

出典と根拠

ORDレコード
ord-f65d1ac51a354ca2a96438f6958d1f65
出典データセット
uspto-grants-1990_11
特許番号
US04973738

関連ノート

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