1-Bromo-3-chloropropane → HCID 85711135、化合物

HRID 1075404

反応式

HRID 1075404 の反応式
[CH3:1][N:2]([CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9])[CH3:3].[Br:10][CH2:11][CH2:12][CH2:13][Cl:14]>CO>[Br-:10].[Cl:14][CH2:13][CH2:12][CH2:11][N+:2]([CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9])([CH3:3])[CH3:1]

参加物

4

反応物 2

HCID 80061-Bromo-3-chloropropaneHCID 78090N,N-Dimethylhexylamine

生成物 1

HCID 85711135HCID 85711135、化合物

試薬・触媒・溶媒 1

HCID 887Methanol溶媒

反応条件

温度
65 °C

実験手順

A 500 mL, 3-necked, round-bottomed flask equipped with air condensers and a magnetic stirring plate was charged with N,N-dimethylhexylamine (199.46 grams, 1.54 moles), 1-bromo-3-chloropropane (243.00 grams, 1.54 moles) and 250 mL of methanol The reaction was maintained at 65° C. for 24 hours. Solvent was removed by rotary evaporation under reduced pressure to yield a brown, viscous oil. Yield 445.8 grams (1.55 moles, 100%).

後処理

  1. customA 500 mL, 3-necked, round-bottomed flask equipped with air condensers
  2. customSolvent was removed by rotary evaporation under reduced pressure
  3. customto yield a brown, viscous oil

出典と根拠

ORDレコード
ord-baddc76a16574c178672bdf5acd2d27b
出典データセット
uspto-grants-1999_05
特許番号
US05900475

関連ノート

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