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Lithium sulfate → Glucosamine sulfate lithium chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Lithium sulfate | HCID 66320 | — |
| 反応物 | (3R,4R,5S,6R)-3-amino-6-(hydroxymethyl)oxane-2,4,5-triol hydrochloride | HCID 2723635 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Glucosamine sulfate lithium chloride | HCID 86754062 | — |
反応手順
Example 1 was repeated using 1679 g of purified water, 431.5 g (2 moles) of glucosamine hydrochloride and 128 g (1 mole) of lithium sulfate (monohydrate) instead of the sodium sulfate. After freeze drying, glucosamine sulfate lithium chloride was obtained as a white powder in a yield of 525 g (97% of theoretical).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05902801 |
| 出典データセット | uspto-grants-1999_05 |
| ORD ID | ord-936ee2068b904d9798f028b3ea0fbb36 |
| 出典メモ | uspto-grants-1999_05 |