化工社化工社 化学情報印刷レポート · 研究参考用
Manganese sulfate monohydrate → Glucosamine sulfate manganese chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Manganese sulfate monohydrate | HCID 177577 | — |
| 反応物 | (3R,4R,5S,6R)-3-amino-6-(hydroxymethyl)oxane-2,4,5-triol hydrochloride | HCID 2723635 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Glucosamine sulfate manganese chloride | HCID 86754063 | — |
反応手順
Example 1 was repeated using 450 g of purified water, 107.8 g (0.5 mole) of glucosamine hydrochloride and 42.3 g (0.25 mole) of manganese sulfate monohydrate instead of the sodium sulfate. After freeze drying, glucosamine sulfate manganese chloride was obtained as a white powder in a yield of 144 g (98% of theoretical).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05902801 |
| 出典データセット | uspto-grants-1999_05 |
| ORD ID | ord-045279f9fee44a129807d5810a9ab026 |
| 出典メモ | uspto-grants-1999_05 |