化工社化工社 化学情報印刷レポート · 研究参考用
Water → N-methyl-2H-3-isoquinolone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Water | HCID 962 | — |
| 反応物 | Sodium Bicarbonate | HCID 516892 | — |
| 反応物 | N-methyl-2H-3-isoquinolone sulfate | HCID 21541268 | — |
| 溶媒 | Chloroform | HCID 6212 | — |
| 生成物 | N-methyl-2H-3-isoquinolone | HCID 12435498 | — |
反応手順
70 g. N-methyl-2H-3-isoquinolone sulfate are dissolved, under an atmosphere of nitrogen, in 900 ml. water. 75 g. sodium bicarbonate are added and the mixture is stirred with 500 ml. chloroform. By decantation, there is obtained a chloroform solution of N-methyl-2H-3-isoquinolone, which can be dried over anhydrous sodium sulfate and employed as such or concentrated for a further reaction.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US03954771 |
| 出典データセット | uspto-grants-1976_05 |
| ORD ID | ord-c078a18486cf4a12876c27b719da7b99 |
| 出典メモ | uspto-grants-1976_05 |