Trichloromethanesulfenyl chloride → Methyl[(trichloromethyl)sulfanyl]carbamyl fluoride

反応式

[CH3:1][NH:2][C:3]([F:5])=[O:4].[Cl:6][C:7]([Cl:11])([Cl:10])[S:8]Cl.CCOP(OC1C=CC2C(C)=CC(OC=2C=1)=O)(OCC)=S>>[CH3:1][N:2]([S:8][C:7]([Cl:11])([Cl:10])[Cl:6])[C:3]([F:5])=[O:4]

参加物

反応物 3

HCID 11666Trichloromethanesulfenyl chloride

HCID 10496498O,O-Diethyl O-(4-methyl-2-oxo-2H-1-benzopyran-7-yl) phosphorothioate

HCID 12545956Methylcarbamyl fluoride

生成物 1

HCID 12836648Methyl[(trichloromethyl)sulfanyl]carbamyl fluoride

実験手順

N-Methyl-N-trichloromethanesulfenylcarbamoyl fluoride was prepared from methylcarbamoyl fluoride and trichloromethanesulfenyl chloride according to the method reported in West Germany Pat. No. 1.297,095 (Farbenfabriken Bayer, A. G), June 12, 1969.

出典と根拠

ORDレコード: ord-0388dd647e5a431fb1044755311288ea
出典データセット: uspto-grants-1976_05
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US03956500

反応ノート

読み込み中…

参加物