Dimethylamine → HCID 21536680、化合物

反応式

CNC.[Br:4][C:5]1[C:6]([CH3:17])=[N:7][N:8]([CH:11]([CH2:15][CH3:16])[C:12]([OH:14])=O)[C:9]=1[CH3:10].BrC1[C:23](Br)=[C:22](C)[N:21]([CH:26](C)[C:27](O)=O)N=1>>[Br:4][C:5]1[C:6]([CH3:17])=[N:7][N:8]([CH:11]([CH2:15][CH3:16])[C:12]([N:21]([CH2:26][CH3:27])[CH2:22][CH3:23])=[O:14])[C:9]=1[CH3:10]

参加物

反応物 3

HCID 674Dimethylamine

HCID 21536628HCID 21536628、化合物

HCID 21536642HCID 21536642、化合物

生成物 1

HCID 21536680HCID 21536680、化合物

実験手順

Following the procedure of Example 1, Part C, but substituting diethylamine for dimethylamine and further substituting the 4-bromo-α-ethyl-3,5-dimethylpyrazole-1-acetic acid prepared in Example 60, Part B, above, for the 3,4-dibromo-α,5-dimethylpyrazole-1-acetic acid, there was prepared the corresponding 4-bromo-N,Nα-triethyl-3,5-dimethylpyrazole-1-acetamide having a melting point at 42° to 44° C.

出典と根拠

ORDレコード: ord-5572e46a5aaf41c4a51d40667ffee382
出典データセット: uspto-grants-1976_05
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US03957480

反応ノート

読み込み中…

参加物