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Formaldehyde → N-(morpholinomethylcarbamyl)glycine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Formaldehyde | HCID 712 | — |
| 反応物 | Morpholine | HCID 8083 | — |
| 反応物 | Hydantoic acid | HCID 10020 | — |
| 生成物 | N-(morpholinomethylcarbamyl)glycine | HCID 21537633 | — |
反応手順
1 mol of N-carbamyl glycine and 1 mol of formol are mixed while stirring. This mixture is cooled with ice-bath and 1 mol of morpholine is added slowly while keeping the temperature at about 15°C during 30 feet and at about 50°C during the same time. After cooling the resulting mixture is evaporated until dry. The residue is a white colored paste. The yield of the reaction is 98 %.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US03957774 |
| 出典データセット | uspto-grants-1976_05 |
| ORD ID | ord-a75a564e4b0c4094b9d9dd22f0e9e613 |
| 出典メモ | uspto-grants-1976_05 |