反応式
[NH2:1][C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-:10])=[O:9])=[C:4]([CH3:11])[CH:3]=1.[S:12](=[O:16])(=[O:15])([OH:14])N>>[NH2:1][C:2]1[C:7]([S:12]([OH:16])(=[O:15])=[O:14])=[CH:6][C:5]([N+:8]([O-:10])=[O:9])=[C:4]([CH3:11])[CH:3]=1参加物
3
実験手順
1 mol of 1-amino-3-methyl-4-nitrobenzene, 1,000 ml of one of the solvents indicated below, 198 g of sulphamic acid and the % by volume of catalyst indicated below are reacted analogously to Example 2. The yields of 1-amino-3-methyl-4-nitrobenzene-6-sulphonic acid obtained, and the reaction temperatures are indicated in the table which follows:
後処理
- custombelow are reacted analogously to Example 2
出典と根拠
- ORDレコード
- ord-4b3b5b3bdf5f4a32a8bcb72c491fc38a
- 出典データセット
- uspto-grants-1976_05
- 特許番号
- US03957860
関連ノート
読み込み中…