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Trichloroethylene → 2-METHYL-4,5,alpha,beta-TETRACHLOROSTYRENE
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Trichloroethylene | HCID 6575 | — |
| 反応物 | Benzene, 1,2-dichloro-4-methyl- | HCID 7256 | — |
| 反応物 | Aluminum(III) Chloride | HCID 6451240 | — |
| 生成物 | 2-METHYL-4,5,alpha,beta-TETRACHLOROSTYRENE | HCID 54418847 | — |
反応手順
A mixture containing 131.5 g (1.0 mole), of trichloroethylene, 80.5 (0.5 mole) of 3,4-dichlorotoluene and 5 g. of aluminum chloride was stirred and heated at reflux for 2 hours. The reaction mixture was then washed with concentrated HCl, then with water until neutral, dried and distilled. 42.7 grams of product was collected, having a boiling point of 97°-102°C at 0.5 mm Hg pressure.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US03957891 |
| 出典データセット | uspto-grants-1976_05 |
| ORD ID | ord-d4be8981b50d4d08a51b74a624717a0e |
| 出典メモ | uspto-grants-1976_05 |