Sucrose → HCID 69927845、化合物

HRID 1076820

反応式

HRID 1076820 の反応式
[CH2:1]([OH:23])[C@H:2]1[O:7][C@@H:6]([O:8][C@H:9]2[C@H:13]([OH:14])[C@@:12]([OH:17])([CH2:15][OH:16])[O:11][C@@H:10]2[CH2:18][OH:19])[C@H:5]([OH:20])[C@@H:4]([OH:21])[C@H:3]1[OH:22].[CH2:24]([OH:46])[C@H:25]1[O:30][C@H:29]([O:31][C@:32]2([CH2:41][OH:42])[O:36][C@H:35]([CH2:37][OH:38])[C@@H:34]([OH:39])[C@@H:33]2[OH:40])[C@H:28]([OH:43])[C@@H:27]([OH:44])[C@@H:26]1[OH:45]>>[CH2:24]([OH:46])[C@H:25]1[O:30][C@H:29]([O:31][C@:32]2([CH2:41][OH:42])[O:36][C@H:35]([CH2:37][OH:38])[C@@H:34]([OH:39])[C@@H:33]2[OH:40])[C@H:28]([OH:43])[C@@H:27]([OH:44])[C@@H:26]1[OH:45].[CH2:1]([OH:23])[C@H:2]1[O:7][C@@H:6]([O:8][C@H:9]2[C@H:13]([OH:14])[C@@:12]([OH:17])([CH2:15][OH:16])[O:11][C@@H:10]2[CH2:18][OH:19])[C@H:5]([OH:20])[C@@H:4]([OH:21])[C@H:3]1[OH:22]

参加物

3

反応物 2

HCID 5988SucroseHCID 11333Lactulose

生成物 1

HCID 69927845HCID 69927845、化合物

実験手順

A mixture of lactitol in fine powder, from 100 to 50 mesh, and air, in a mixing ratio of 10-20%, v/v, is injected from the center nozzle of a two-fluid nozzle attached on the top of a spray-drying tower. Separately, a 75% aqueous sucrose solution which is cooled gradually with agitation and which is beginning to crystallize is sprayed through the outer nozzle applying a pressure of 50 to 100 kg/cm2 to allow the sprayed solution to contact with powderd lactitol and then the mixture is dried with hot air charged from the top of the drying tower. Alternatively, a sucrose solution as described above may be sprayed on a horizontal fluidized-bed of lactitol fine powder, and the lactitol powder and the sucrose drops may be dried as a whole to obtain a crystalline sucrose-lactitol product. The mixing ratio of sucrose and lactitol is adjusted to meet the degree required for the product as table sugar.

後処理

  1. customto crystallize
  2. customthe mixture is dried with hot air
  3. additioncharged from the top of the drying tower
  4. dry with materialthe lactitol powder and the sucrose drops may be dried as a whole

出典と根拠

ORDレコード
ord-358285e0a44d44b999644764a1a6613a
出典データセット
uspto-grants-1976_05
特許番号
US03957976

関連ノート

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