関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Oxalic Acid | HCID 971 | — |
| 反応物 | HCID 178419084 | HCID 178419084 | — |
| 触媒 | Niobium potassium oxide | HCID 160967 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | HCID 178526029 | HCID 178526029 | — |
反応手順
Granulated alumina (8 - 16 mesh) is heated at 1300°C. for 4 hours. Potassium niobate (4K2O.3Nb2O5.16H2O) and vanadium pentoxide are suspended in 5 parts of water, heated to 80°C., and oxalic acid is added slowly to obtain a blue-colored vanadium oxalate solution. Sodium carbonate is added and the alumina is also placed in the solution. The mixture is dried over a water bath with agitation. While air is pumped in, it is indurated in a furnace at 400°C. for 16 hours to obtain the catalyst ready for use after cooling.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US03959336 |
|---|
| 出典データセット | uspto-grants-1976_05 |
|---|
| ORD ID | ord-a044738a2e224cfe80529a948e354241 |
|---|
| 出典メモ | uspto-grants-1976_05 |
|---|
