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HRID 1077457作成日:2026年10月27日

2,3-Dimethoxycinnamic acid → 1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(2,3-dimethoxyphenyl)ethenyl)-1,3-dipropyl-, (E)-

https://huagongshe.com/reaction/1077457

反応式

関与物質

役割名称HCID仕込み量
反応物2,3-Dimethoxycinnamic acidHCID 99525—
反応物5,6-Diamino-1,3-dipropyl-2,4(1H,3H)-pyrimidinedioneHCID 5098605—
生成物1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(2,3-dimethoxyphenyl)ethenyl)-1,3-dipropyl-, (E)-HCID 644878436%

反応手順

Substantially the same procedure as in Reference Example 1 was repeated using 2.0 g (8.85 mmol) of 5,6-diamino-1,3-dipropyluracil and 2.2 g (10.6 mmol) of 2,3-dimethoxycinnamic acid. Then, the resultant crude crystals were recrystallized from chloroform/cyclohexane to give 1.26 g (yield 36%) of Compound 29 as yellow crystals.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05543415
出典データセットuspto-grants-1996_08
ORD IDord-53a531af42fe472fbf57f7c9a41a036d
出典メモuspto-grants-1996_08