化工社化工社 化学情報印刷レポート · 研究参考用
Phenyltrichlorosilane → Dichlorodiphenylsilane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Phenyltrichlorosilane | HCID 7372 | — |
| 反応物 | Triethylamine | HCID 8471 | — |
| 触媒 | Dichloro(phenyl)silane | HCID 74207 | — |
| 溶媒 | Benzene | HCID 241 | — |
| 生成物 | Dichlorodiphenylsilane | HCID 6627 | 253.1% |
反応手順
Triethylamine (3.9 g) was added to a flask containing 83.3 g of the crude product mixture described in Example 1. This mixture was stripped by the process described in Example 1. The volatiles were condensed and analyzed by GC-TCD. About 77.4 g of a liquid was recovered comprising 24.7 g of diphenyldichlorosilane (yield of 77 percent), 1.4 g of phenyldichlorosilane, 24.5 g of phenyltrichlorosilane, and 10.1 g of benzene.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05545743 |
| 出典データセット | uspto-grants-1996_08 |
| ORD ID | ord-7290619a4c9d4a31a80dd0728247d398 |
| 出典メモ | uspto-grants-1996_08 |