1,3-Butadiene → 3-Methoxytoluene

HRID 1079088ノート

反応式

HRID 1079088 の反応式
C=CC=C.[CH3:5][O:6][C:7]1[CH:8]=[C:9]([CH2:13]CC=CC)[CH:10]=[CH:11][CH:12]=1>O>[CH3:5][O:6][C:7]1[CH:8]=[C:9]([CH3:13])[CH:10]=[CH:11][CH:12]=1

参加物

4

反応物 2

HCID 78451,3-ButadieneHCID 54500863HCID 54500863、化合物

生成物 1

HCID 75303-Methoxytoluene収率 79%

試薬・触媒・溶媒 1

HCID 962Water溶媒

反応条件

温度
110 °C

実験手順

After the flask was heated at a temperature of 110° C. during stirring in order to disperse the catalysts, 1,3-butadiene was fed for 6 hours at a flow rate of 0.3 mol/hour in order to promote the addition reaction. After the completion of the reaction, water was added to deactivate and separate the catalysts. The thus obtained reaction mixture was analyzed by gas chromatography. The results indicated that 5-(3-methoxyphenyl)-2-pentene was produced at 79% yield with respect to the consumed m-methoxytoluene.

後処理

  1. additionthe addition reaction
  2. additionwas added to deactivate and
  3. customseparate the catalysts
  4. customThe thus obtained reaction mixture

出典と根拠

ORDレコード
ord-336e05441973463c9caf17c37b31a4a0
出典データセット
uspto-grants-1996_08
特許番号
US05550284

反応ノート

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