1-Propene-1,1,3-tricarbonitrile, 2-phenyl- → 3-[[4-(Diethylamino)phenyl]imino]-2-phenyl-1-propene-1,1,3-tricarbonitrile

反応式

[C:1]1([C:7]([CH2:13][C:14]#[N:15])=[C:8]([C:11]#[N:12])[C:9]#[N:10])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH2:16]([N:20]([CH2:29][CH2:30]CC)[C:21]1[CH:26]=[CH:25][C:24]([N:27]=O)=[CH:23][CH:22]=1)[CH2:17]CC>>[CH2:29]([N:20]([CH2:16][CH3:17])[C:21]1[CH:26]=[CH:25][C:24]([N:27]=[C:13]([C:14]#[N:15])[C:7]([C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)=[C:8]([C:11]#[N:12])[C:9]#[N:10])=[CH:23][CH:22]=1)[CH3:30]

参加物

反応物 2

HCID 46214401-Propene-1,1,3-tricarbonitrile, 2-phenyl-

HCID 13843803N,N-dibutyl-p-nitrosoaniline

生成物 1

HCID 233554853-[[4-(Diethylamino)phenyl]imino]-2-phenyl-1-propene-1,1,3-tricarbonitrile

実験手順

The above procedure was used for the preparation of 3-[[4-dibutylamino)phenyl]imino]-2-phenyl-1-propene-1,1,3-tricarbonitrile using N,N-dibutyl-4-nitrosoaniline in place of N,N-diethyl-4-nitrosoaniline.

出典と根拠

ORDレコード: ord-38924de5781742998f161ae7a2808fa7
出典データセット: uspto-grants-1996_12
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US05583178

反応ノート

読み込み中…