2-Chloromethyl-4-(2-furylmethylthio)-3-methylpyridine hydrochloride → HCID 178431892、化合物
反応式
[ClH:1].[Cl:2][CH2:3][C:4]1[C:9]([CH3:10])=[C:8]([S:11][CH2:12][C:13]2[O:14][CH:15]=[CH:16][CH:17]=2)[CH:7]=[CH:6][N:5]=1.[SH:18][C:19]1[NH:23][C:22]2[CH:24]=[CH:25][C:26]([C:28]([F:31])([F:30])[F:29])=[CH:27][C:21]=2[N:20]=1>C(O)(C)C>[ClH:2].[ClH:1].[O:14]1[CH:15]=[CH:16][CH:17]=[C:13]1[CH2:12][S:11][C:8]1[CH:7]=[CH:6][N:5]=[C:4]([CH2:3][S:18][C:19]2[NH:23][C:22]3[CH:24]=[CH:25][C:26]([C:28]([F:31])([F:30])[F:29])=[CH:27][C:21]=3[N:20]=2)[C:9]=1[CH3:10]参加物
4
実験手順
Following the procedure described in Example 12, the reaction of 2-chloromethyl-4-(2-furylmethylthio)-3-methylpyridine hydrochloride with 2-mercapto-5-trifluoromethyl-1H-benzimidazole in isopropanol gives the title compound as a colorless solid; m.p. 173° C (decomp.).