Hexacyanocobalt → HCID 11125012、化合物

HRID 1082039ノート

反応式

HRID 1082039 の反応式
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参加物

4

反応物 2

HCID 407334HexacyanocobaltHCID 3007855Zincchloride

生成物 1

HCID 11125012HCID 11125012、化合物

試薬・触媒・溶媒 1

HCID 962Water溶媒3 回

実験手順

Potassium hexacyanocobaltate (4.0 g) is dissolved in deionized water (150 mL) in a beaker. Zinc chloride (10 g) is dissolved in deionized water (15 mL) in a second beaker. The aqueous solutions are quickly combined and magnetically stirred for 10 min. The precipitated solids are isolated by centrifugation. The solids are reslurried in deionized water (100 mL) for 10 min. with stirring, and are again recovered by centrifugation. The catalyst is dried in a vacuum oven at 50° C. and 30 in. (Hg) to constant weight. This catalyst is identified as Catalyst A.

後処理

  1. customThe precipitated solids are isolated by centrifugation
  2. stirringwith stirring
  3. customare again recovered by centrifugation
  4. customThe catalyst is dried in a vacuum oven at 50° C.

出典と根拠

ORDレコード
ord-1c1f0b0828a34273a86f31da1936f38b
出典データセット
uspto-grants-1996_12
特許番号
US05589431

反応ノート

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