化工社化工社 化学情報印刷レポート · 研究参考用
HRID 1082893作成日：2026年10月26日
1-Methyl-1H-imidazole-4-carbonitrile → ethyl 4-(4-cyano-1-methyl-1H-imidazol-5-yl)-1-ethyl-1H-pyrrole-2-carboxylate
https://huagongshe.com/reaction/1082893
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 1-Methyl-1H-imidazole-4-carbonitrile | HCID 2795115 | — |
| 反応物 | Ethyl 4-bromo-1-ethyl-1H-pyrrole-2-carboxylate | HCID 78918332 | — |
| 試薬 | Potassium Trimethylacetate | HCID 23662159 | — |
| 触媒 | Benzenamine, 4-(dicyclohexylphosphino)-N,N-dimethyl- | HCID 142458 | — |
| 触媒 | HCID 178455864 | HCID 178455864 | — |
| 溶媒 | Dimethylacetamide | HCID 31374 | — |
| 生成物 | ethyl 4-(4-cyano-1-methyl-1H-imidazol-5-yl)-1-ethyl-1H-pyrrole-2-carboxylate | HCID 117937785 | 10.35% |
| 内部標準 | 4,4'-Bis(1,1-dimethylethyl)-1,1'-biphenyl | HCID 74195 | — |
情報源と証拠
| DOI | 10.26434/chemrxiv |
|---|
| 出典データセット | Pd-catalyzed C-H arylation of imidazole with aryl bromide |
|---|
| ORD ID | ord-0b71c7a1c6dd4a6a8cf4ff4fa338d963 |
|---|
| 出典メモ | Pd-catalyzed C-H arylation of imidazole with aryl bromide |
|---|
