化工社化工社 化学情報印刷レポート · 研究参考用
Ethyl Acetoacetate → Ethyl 3-tetrahydropyrrolyl-2-butenoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl Acetoacetate | HCID 8868 | — |
| 反応物 | Pyrrolidine | HCID 31268 | — |
| 生成物 | Ethyl 3-tetrahydropyrrolyl-2-butenoate | HCID 69630519 | — |
反応手順
Ethyl 3-tetrahydropyrrolyl-2-butenoate was prepared (21 g, 99%) from ethyl acetoacetate (15.0 g, 115.26 mmol) and pyrrolidine (71.1 mL, 345.78 mmol) in the same manner as described in the above Example 1 (1), and the obtained product was identified with the following NMR data.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07094908B2 |
| 出典データセット | uspto-grants-2006_08 |
| ORD ID | ord-c4f6c0a039404fa9b84557e51bc4c6bf |
| 出典メモ | uspto-grants-2006_08 |