化工社化工社 化学情報印刷レポート · 研究参考用
Pyrrolidine → Allyl 3-tetrahydropyrrolyl-2-butenoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Pyrrolidine | HCID 31268 | — |
| 反応物 | Allyl acetoacetate | HCID 70701 | — |
| 生成物 | Allyl 3-tetrahydropyrrolyl-2-butenoate | HCID 69629910 | — |
反応手順
Allyl 3-tetrahydropyrrolyl-2-butenoate was prepared (4.7 g, 68%) in the same manner as described in the above Example 1 (1) from allyl acetoacetate (5.0 g, 35.17 mmol) and pyrrolidine (8.8 mL, 105.51 mmol), and the obtained product was identified with the following 1H NMR data.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07094908B2 |
| 出典データセット | uspto-grants-2006_08 |
| ORD ID | ord-b23c8ba54c484e1bafaf208e0e2e4633 |
| 出典メモ | uspto-grants-2006_08 |