化工社化工社 化学情報印刷レポート · 研究参考用
Triethylamine → Diethyl 3-phenyl-2-isoxazolin-5-ylmethylphosphonate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Triethylamine | HCID 8471 | — |
| 反応物 | (Z)-Benzaldehyde oxime | HCID 12143 | — |
| 反応物 | Chlorosuccinimide | HCID 31398 | — |
| 反応物 | Diethyl allylphosphonate | HCID 573014 | — |
| 生成物 | Diethyl 3-phenyl-2-isoxazolin-5-ylmethylphosphonate | HCID 20062399 | — |
反応手順
In analogy to Example 1, 76.7 g of an oily crude product are obtained starting from 30.3 g (0.25 mol) of benzaldoxime, 36.7 g (0.275 mol) of N-chlorosuccinimide, 49 g (0.275 mol) of diethyl allylphosphonate and 38.2 ml (0.275 mol) of triethylamine and can be purified as described in Example 1.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05006515 |
| 出典データセット | uspto-grants-1991_04 |
| ORD ID | ord-9ec388885fd14ede8f3fc57e3c0d5276 |
| 出典メモ | uspto-grants-1991_04 |