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Triethylamine → Dimethyl 3-(3-phenoxyphenyl}-2-isoxazolin-5-ylphosphonate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Triethylamine | HCID 8471 | — |
| 反応物 | Chlorosuccinimide | HCID 31398 | — |
| 反応物 | Dimethyl vinylphosphonate | HCID 78376 | — |
| 反応物 | N-[(3-phenoxyphenyl)methylidene]hydroxylamine | HCID 2393595 | — |
| 生成物 | Dimethyl 3-(3-phenoxyphenyl}-2-isoxazolin-5-ylphosphonate | HCID 20062400 | 95.6% |
反応手順
In analogy to Example 1, 42.65 g (0.2 mol) of 3-phenoxybenzaldoxime, 29.4 g (0.22 mol) of N-chlorosuccinimide, 29.2 ml (0.22 mol) of dimethyl vinylphosphonate and 30.6 ml (0.22 mol) of triethylamine are reacted, and 66.4 g of oily product are obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05006515 |
| 出典データセット | uspto-grants-1991_04 |
| ORD ID | ord-c8cfc1ea41c640a39693d56401eb3774 |
| 出典メモ | uspto-grants-1991_04 |