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Triethylamine → Dimethyl 3-(1-naphthyl)-2-isoxazolin-5-ylphosphonate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Triethylamine | HCID 8471 | — |
| 反応物 | Chlorosuccinimide | HCID 31398 | — |
| 反応物 | Dimethyl vinylphosphonate | HCID 78376 | — |
| 反応物 | 1-Naphthalenecarboxaldehyde, oxime | HCID 240801 | — |
| 生成物 | Dimethyl 3-(1-naphthyl)-2-isoxazolin-5-ylphosphonate | HCID 20062404 | — |
反応手順
Preparation is carried out in analogy to Example 1 from 31.2 g (0.2 mol) of 1-naphthaldoxime, 29.4 g (0.22 mol) of N-chlorosuccinimide, 29.2 ml (0.22 mol) of dimethyl vinylphosphonate and 30.6 ml (0.22 mol) of triethylamine, with 56 g of oily compound being obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05006515 |
| 出典データセット | uspto-grants-1991_04 |
| ORD ID | ord-c8375bb701b14142941725e3d7153d4e |
| 出典メモ | uspto-grants-1991_04 |