関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | p-Fluoronitrobenzene | HCID 9590 | — |
| 反応物 | 1,4,7-Trimethyldiethylenetriamine | HCID 66930 | — |
| 溶媒 | Dimethyl Sulfoxide | HCID 679 | — |
| 生成物 | N,N', N"-trimethyl-N-(4-nitrophenyl)diethylenetriamine | HCID 21625360 | — |
反応手順
In 7 ml of dimethyl sulfoxide were dissolved 1.41 g of p-fluoronitrobenzene and 14 g of N,N',N"-trimethyldiethylenetriamine, and the mixture was then stirred at 120° C. for 3 hours.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05008267 |
|---|
| 出典データセット | uspto-grants-1991_04 |
|---|
| ORD ID | ord-ea800a3811824a62a5c3612ba298168a |
|---|
| 出典メモ | uspto-grants-1991_04 |
|---|
