関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Sulfuric Acid | HCID 1118 | — |
| 反応物 | O-Terphenyl | HCID 6766 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | HCID 131716827 | HCID 131716827 | — |
反応手順
880 g of concentrated sulfuric acid were heated to 110° C, and 270.5 g of terphenyl were added. The temperature was raised to 140° C and left on that level for 4 hours. After cooling down to 100° C, 800 ml of water were added dropwise, and the mixture was allowed to cool and then filtered with suction, giving a crude product which was used direct in the next stage. Purity (HPLC): 99.7%; yield: 565 g.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05008472 |
|---|
| 出典データセット | uspto-grants-1991_04 |
|---|
| ORD ID | ord-2042710a350c43b99826428d2aed046a |
|---|
| 出典メモ | uspto-grants-1991_04 |
|---|
