2-Phenoxybenzoic acid hydrazide → HCID 53690311、化合物
反応式
[N:1]1[CH:6]=[CH:5][C:4]([C:7]([CH2:9][CH:10]([CH3:12])[CH3:11])=O)=[CH:3][CH:2]=1.[O:13]([C:20]1[CH:29]=[CH:28][CH:27]=[CH:26][C:21]=1[C:22]([NH:24][NH2:25])=[O:23])[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1>C(O)(=O)C>[CH3:11][CH:10]([CH3:12])[CH2:9][C:7](=[N:25][NH:24][C:22](=[O:23])[C:21]1[CH:26]=[CH:27][CH:28]=[CH:29][C:20]=1[O:13][C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)[C:4]1[CH:5]=[CH:6][N:1]=[CH:2][CH:3]=1参加物
4
実験手順
Following the general method of procedure 4 and making noncritical variations, except 12 drops of glacial acetic acid is added as a catalyst, 9.00 gm (0.055 mole) of isobutyl 4-pyridyl ketone and 12.59 gm (0.055 mole) of 2-phenoxybenzhydrazide yield 13.89 gm (67%) of the title compound having a melting point of 137.6° C.
出典と根拠
- ORDレコード