化工社化工社 化学情報印刷レポート · 研究参考用
N-(2-Hydroxyethyl)ethylenediamine → Octyl hydroxyethyl imidazoline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N-(2-Hydroxyethyl)ethylenediamine | HCID 8112 | — |
| 反応物 | Nonanenitrile | HCID 16715 | — |
| 溶媒 | Carbon Disulfide | HCID 6348 | — |
| 生成物 | Octyl hydroxyethyl imidazoline | HCID 117550 | 62.7% |
反応手順
13.02 g (93.51 mmoles) of octyl cyanide was treated with 12.327 g (118.36 mmoles) of 2-(2-aminoethylamino)ethanol in presence of 0.5 ml of carbon disulfide at 125° C. for 24 hrs. and worked up as outlined under Example 23. Distillation of the residue at 167°-169° C./0.5 mm gave 12.332 g (62.7%) of product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05030629 |
| 出典データセット | uspto-grants-1991_07 |
| ORD ID | ord-8aa60d48881043c1aec24d3113c0485e |
| 出典メモ | uspto-grants-1991_07 |