化工社化工社 化学情報印刷レポート · 研究参考用
Ethyl Dodecanoate → 1-(4-Hydroxybutyl)-2-undecyl-2-imidazoline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl Dodecanoate | HCID 7800 | — |
| 反応物 | 1-Butanol, 4-[(2-aminoethyl)amino]- | HCID 22184070 | — |
| 溶媒 | Hexane | HCID 8058 | — |
| 生成物 | 1-(4-Hydroxybutyl)-2-undecyl-2-imidazoline | HCID 15158283 | 54.2% |
反応手順
8 g (60.6 mmoles) of 4-(2-aminoethylamino)butanol and 12.5 g of ethyl dodecanoate were treated as under Example 25. The resulting 10.8 g of an oil (66.7%) was dissolved in 100 ml of hexane and kept in the freezer to give 8.8 g of pure product, m.p. 58°-60° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05030629 |
| 出典データセット | uspto-grants-1991_07 |
| ORD ID | ord-ef8fe471127f454bbf9c0b33feba8bc8 |
| 出典メモ | uspto-grants-1991_07 |