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Hexanenitrile → HCID 178442284、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hexanenitrile | HCID 12352 | — |
| 反応物 | 2-Methylpropylenediamine | HCID 13128 | — |
| 溶媒 | Carbon Disulfide | HCID 6348 | — |
| 生成物 | HCID 178442284 | HCID 178442284 | 73.4% |
反応手順
8.41 g (95.4 mmoles) of 1,2-diamino-2-methylpropane, 7.4 g (76.16 mmoles) of hexanenitrile and 0.4 ml of carbon disulfide were heated at 125° C. for 24 hours and then worked up as under Example 23. Distillation at 105°-107° C./0.5 mm gave 9.4 g (73.4%) of product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05030629 |
| 出典データセット | uspto-grants-1991_07 |
| ORD ID | ord-774414b09cb54582b80ce98d82d5fa71 |
| 出典メモ | uspto-grants-1991_07 |