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4-(Octyloxy)benzoic acid → 4-Octyloxybenzoyl chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-(Octyloxy)benzoic acid | HCID 17231 | — |
| 反応物 | Phosphorus pentachloride | HCID 24819 | — |
| 溶媒 | Benzene | HCID 241 | — |
| 生成物 | 4-Octyloxybenzoyl chloride | HCID 2760250 | — |
反応手順
2.78 g of 4-octyloxybenzoic acid was added to 10 ml of benzene, and under stirring at room temperature, 2.36 g of PCl5 was added little by little. The mixture was then heated under reflux for 4 hours. Thereafter, the solvent was distilled off to obtain 4-octyloxybenzoic acid chloride.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05034152 |
| 出典データセット | uspto-grants-1991_07 |
| ORD ID | ord-d0c650b3ad4245688f41bd261bc78567 |
| 出典メモ | uspto-grants-1991_07 |