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Epichlorohydrin → 3-(1-Bromonaphth-2-yloxy)-1,2-epoxypropane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Epichlorohydrin | HCID 7835 | — |
| 反応物 | 1-Bromo-2-naphthol | HCID 11316 | — |
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 溶媒 | Methyl Ethyl Ketone | HCID 6569 | — |
| 生成物 | 3-(1-Bromonaphth-2-yloxy)-1,2-epoxypropane | HCID 14369942 | — |
反応手順
A suspension containing 22.3 g of 1-bromonaphth-2-ol, 27.75 g of 1-chloro-2,3-epoxypropane and 27.6 g of potassium carbonate in 200 ml of butanone is refluxed overnight. The inorganic salts are filtered off and drained and the filtrate is then evaporated under vacuum. The oil obtained is distilled under 0.01 mm of mercury.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05036077 |
| 出典データセット | uspto-grants-1991_07 |
| ORD ID | ord-e743b44489f04654891d9a3d50b33511 |
| 出典メモ | uspto-grants-1991_07 |