1-(2-Methoxyphenyl)piperazine → HCID 14556334、化合物
反応式
[CH3:1][N:2]1[C:6]2[CH:7]=[CH:8][C:9]([C:11](=[O:15])[C:12](=[CH2:14])[CH3:13])=[CH:10][C:5]=2[O:4][C:3]1=[O:16].[CH3:17][O:18][C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][C:20]=1[N:25]1[CH2:30][CH2:29][NH:28][CH2:27][CH2:26]1>CC(C)=O>[CH3:1][N:2]1[C:6]2[CH:7]=[CH:8][C:9]([C:11](=[O:15])[CH:12]([CH3:13])[CH2:14][N:28]3[CH2:27][CH2:26][N:25]([C:20]4[CH:21]=[CH:22][CH:23]=[CH:24][C:19]=4[O:18][CH3:17])[CH2:30][CH2:29]3)=[CH:10][C:5]=2[O:4][C:3]1=[O:16]参加物
4
実験手順
100 cm3 of anhydrous acetone, 0.01 mole of 3-methyl-6-(2-methylenepropionyl)benzoxazolinone and 0.01 mole of 1-(2-methoxyphenyl)piperazine are introduced successively into a 250-cm3 ground-necked flask equipped with a reflux condenser and a magnetic stirrer. The mixture is brought to reflux for 6 hours and allowed to cool. The product is drained: the product of the title is obtained.
後処理
- customequipped with a reflux condenser and a magnetic stirrer