関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Octacosanoic acid | HCID 10470 | — |
| 反応物 | Neopentyl glycol | HCID 31344 | — |
| 反応物 | Tin atom | HCID 5352426 | — |
| 生成物 | Neopentyl glycol monomontanate | HCID 85568373 | — |
反応手順
64.2 g neopentyl glycol (0.617 mole), 246.9 g montanic acid (0.617 mole) and 0.4 g tin powder were heated to 210° C. as in Example 1 with application of a gentle vacuum. The vacuum was increased to 150 mbar over a period of 5 h. The product had an acid number of approximately 2. A brown-yellow hard wax having a dropping point of 72° C. was obtained after cooling to 100° C., bleaching and filtering.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04962145 |
|---|
| 出典データセット | uspto-grants-1990_10 |
|---|
| ORD ID | ord-6a38810761a14ba0b783290ca92ba777 |
|---|
| 出典メモ | uspto-grants-1990_10 |
|---|
