関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Sorbitol | HCID 5780 | — |
| 反応物 | Octacosanoic acid | HCID 10470 | — |
| 反応物 | Tin atom | HCID 5352426 | — |
| 生成物 | Sorbitol trimontanate | HCID 86744265 | — |
反応手順
41.1 g sorbitol (0.226 mole), 271.1 g montanic acid (0.678 mole) and 0.4 g tin powder were heated to 200° C. as in Example 1 with application of a gentle vacuum. The vacuum was increased to 15 mbar over a period of 14 h, by which time the acid value had fallen to 5. After cooling to 100° C., the product was filtered, giving a brown hard wax having a dropping point of 78° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04962145 |
|---|
| 出典データセット | uspto-grants-1990_10 |
|---|
| ORD ID | ord-ad12c830b0954be2b0ad1e72ee90f6ba |
|---|
| 出典メモ | uspto-grants-1990_10 |
|---|
