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Acrylic Acid → Ethylacrylate acrylic acid acrylonitrile
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acrylic Acid | HCID 6581 | — |
| 反応物 | Acrylonitrile | HCID 7855 | — |
| 反応物 | 1-Dodecanethiol | HCID 8195 | — |
| 反応物 | Ethyl Acrylate | HCID 8821 | — |
| 反応物 | Lauryl peroxide | HCID 76169 | — |
| 反応物 | Butyl perbenzoate | HCID 83282 | — |
| 溶媒 | O-Xylene | HCID 7237 | — |
| 生成物 | Ethylacrylate acrylic acid acrylonitrile | HCID 168852 | — |
反応手順
this polymer material was produced by adding to 320 g xylene at 100° C. the monomer solution and a catalyst solution over a period of 3 hours. The monomer solution contained 2.900 g ethyl acrylate, 76 g acrylonitrile, 76 g acrylic acid and 3 g laurylmercaptan. The catalyst solution contained 26 g laurylperoxide and 7 g butylperbenzoate in 273 g of xylene. The material was highly viscous with comonomer proportions of 95:2.5:2.5.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04965117 |
| 出典データセット | uspto-grants-1990_10 |
| ORD ID | ord-3302c6cf61fb48c19c71da6e8611e7f0 |
| 出典メモ | uspto-grants-1990_10 |