反応式
C[Si]([CH2:5][C:6]([O-:8])=[O:7])(C)C.Cl[Si:10]1(Cl)[CH2:13][CH2:12][CH2:11]1>>[C:6]([O:8][Si:10]1([O:8][C:6](=[O:7])[CH3:5])[CH2:13][CH2:12][CH2:11]1)(=[O:7])[CH3:5]参加物
3
反応条件
- 温度
- 25 °C
実験手順
To 30.0 g trimethylsilylacetate was added 16.0 g 1,1-dichlorosilacyclobutane. The reactants were stirred for one hour at 25 ° C. and fractional distillation performed on the reaction mixture. The title compound was isolated as a clear, colorless fluid. The yield was 14.6 g (81.4%). The structure of the product was confirmed by mass spectroscopy and nuclear magnetic resonance spectroscopy (NMR).
後処理
- distillationfractional distillation
出典と根拠
- ORDレコード
- ord-f4d327f92e4a4de5b56a0b7b9b71e94e
- 出典データセット
- uspto-grants-1990_10
- 特許番号
- US04965367
関連ノート
読み込み中…