Toluene → HCID 23693107、化合物

HRID 1089641

反応式

HRID 1089641 の反応式
C(OC)(=O)C1C=CC(C([O-])=O)=CC=1.[K+:14].[C:15]([O:28]CC)(=[O:27])[C:16]1[CH:26]=[CH:25][C:19]([C:20]([O:22][CH2:23][CH3:24])=[O:21])=[CH:18][CH:17]=1.[OH-].[K+].C1(C)C=CC=CC=1>C(O)C>[C:20]([O:22][CH2:23][CH3:24])(=[O:21])[C:19]1[CH:25]=[CH:26][C:16]([C:15]([O-:28])=[O:27])=[CH:17][CH:18]=1.[K+:14]

参加物

6

反応物 4

HCID 1140TolueneHCID 12483Diethyl terephthalateHCID 14797Potassium HydroxideHCID 236837531,4-Benzenedicarboxylic acid, 1-methyl ester, potassium salt (1:1)

生成物 1

HCID 23693107HCID 23693107、化合物

試薬・触媒・溶媒 1

HCID 702Ethanol溶媒

実験手順

This compound was prepared by the procedure described for potassium monomethyl terephthalate. Typical reagent levels were as follows: 77.0 gm (0.346 mole) of diethyl terephthalate, 19.4 gm of potassium hydroxide, 150 ml of toluene and 100 ml of ethanol.

後処理

  1. customThis compound was prepared by the procedure

出典と根拠

ORDレコード
ord-6fc1ab55849247b0a645d3cb5ff02d94
出典データセット
uspto-grants-1992_01
特許番号
US05078907

関連ノート

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