化工社化工社 化学情報印刷レポート · 研究参考用
1-Hexanol → 1,4-Benzenedicarboxylic acid, 1-methyl ester, potassium salt (1:1)
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Hexanol | HCID 8103 | — |
| 反応物 | Potassium Hydroxide | HCID 14797 | — |
| 反応物 | Dihexyl terephthalate | HCID 519527 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | 1,4-Benzenedicarboxylic acid, 1-methyl ester, potassium salt (1:1) | HCID 23683753 | — |
反応手順
Typical reagent levels were as follows: dihexyl terephthalate (33.5 g, 0.10 mole), potassium hydroxide (5.6 g, 0.10 mole), 100 ml of toluene and 20 ml of 1-hexanol. After workup 20.2g (70%) of product was recovered.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05078907 |
| 出典データセット | uspto-grants-1992_01 |
| ORD ID | ord-cf7e5e903a6647c694d5ca44036477cf |
| 出典メモ | uspto-grants-1992_01 |